• DOE and Parallel reaction
Optimization of reaction conditions: reagent equivalent, temperature, concentration, reaction time, etc.
These methods can significantly improve the efficiency of condition optimization and quickly achieve optimal conditions.
• Destructive test (Stress test)
It is essential to do destructive tests for laboratory-scale batches, including the stability of starting materials, intermediates and products.
After the initial optimization of the process, it tests the applicable scope of the process.
• The Spiking experiments
Verification of process performance, such as assessing the reasonableness of specification settings and the capability to remove impurities.
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